(1aS,7bS)-2,2-Dimethyl-1a,7b-dihydro-2H-oxireno[2,3-c]chromene-6-carbonitrile → HCID 68644294, compound

HRID 1159624Notes

Reaction equation

HRID 1159624 reaction equation
[CH3:1][C:2]1([CH3:15])[O:11][C:10]2[C:5](=[CH:6][C:7]([C:12]#[N:13])=[CH:8][CH:9]=2)[C@@H:4]2[O:14][C@H:3]12.[CH3:16][O:17][C:18]1[CH:19]=[CH:20][C:21]2[O:25][NH:24][C:23](=[O:26])[C:22]=2[CH:27]=1>>[OH:14][C@H:3]1[C@H:4]([O:26][C:23]2[C:22]3[CH:27]=[C:18]([O:17][CH3:16])[CH:19]=[CH:20][C:21]=3[O:25][N:24]=2)[C:5]2[C:10](=[CH:9][CH:8]=[C:7]([C:12]#[N:13])[CH:6]=2)[O:11][C:2]1([CH3:15])[CH3:1]

Participants

3

Reactant 2

HCID 9837089(1aS,7bS)-2,2-Dimethyl-1a,7b-dihydro-2H-oxireno[2,3-c]chromene-6-carbonitrileHCID 11457875HCID 11457875, compound

Product 1

HCID 68644294HCID 68644294, compound

Procedure

Following the procedure in Example 1, using (S,S)-2,2-dimethyl-1a,7b-dihydro-2H-1,3-dioxa-cyclopropa[a]naphthalene-6-carbonitrile and 5-methoxy-benzo[d]isoxazol-3-one as starting materials, the title compound was prepared as a white solid.

Sources & evidence

ORD record
ord-9c8615f5a0284253b9e7a0604ee08389
Source dataset
uspto-grants-2010_10
Patent number
US07812183B2

Reaction notes

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