HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Methoxy-m-toluenesulfonyl chloride → 4-Bromo-1-[(2-methoxy-5-methylphenyl)sulfonyl]-1H-indole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Methoxy-m-toluenesulfonyl chloride | HCID 145149 | — |
| Reactant | 4-Bromo-1-(toluene-4-sulfonyl)-1H-indole | HCID 562869 | — |
| Product | 4-Bromo-1-[(2-methoxy-5-methylphenyl)sulfonyl]-1H-indole | HCID 68716840 | — |
Reaction Steps
The procedure for Intermediate 3 was followed using (2-methoxy-5-methylphenyl)sulfonyl chloride. Yield 1.4 g (72%). MS (ESI+) for C16H14BrNO3S m/z 382 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07812017B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-b5096f3a8d1e4e658724f6b636ebf32a |
| Source note | uspto-grants-2010_10 |