HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tributylvinyltin → HCID 68714627, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tributylvinyltin | HCID 81998 | — |
| Reactant | HCID 68713053 | HCID 68713053 | — |
| Reactant | 4-Bromo-1-(2-thienylsulfonyl)-1H-indole | HCID 68717174 | — |
| Product | HCID 68714627 | HCID 68714627 | 79% |
Reaction Steps
The experimental for Intermediate 15 was followed using 4-bromo-1-(2-thienylsulfonyl)-1H-indole (500 mg, 1.46 mmol; Intermediate 20), tributyl(vinyl)stannane (tot 0.864 mL, 2.92 mmol) and Pd(PPh3)2OAc2 (tot 55 mg, 0.073 mmol). The title compound (333 mg, 79%) was obtained as a colorless solid. MS (ESI+) for C14H11NO2S2 m/z 290 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07812017B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-2be5bb3e7575490d9f1d693412a3b897 |
| Source note | uspto-grants-2010_10 |