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HRID1159934

反应详情

EQUATION

反应方程式

HRID 1159934 的结构方程式

REACTANTS

反应物

2
结构：CN(C)CCOc1ccc(Nc2nccc(-c3c(-c4cccc(NC(=O)c5c(F)cccc5F)c4)nn4ccccc34)n2)cc1Cl
HCID11505567

未命名化合物

结构：COCCOc1ccc([N+](=O)[O-])cc1F
HCID23498075

未命名化合物

PRODUCTS

生成物

1
结构：COCCOc1ccc(N)cc1F
HCID23498117

3-Fluoro-4-(2-methoxyethoxy)aniline

C9H12FNO2

PROCEDURE

实验过程

In a procedure analogous to Example 125, 250 mg of the title compound was prepared from 2-fluoro-1-{[2-(methyloxy)ethyl]oxy}-4-nitrobenzene as brown oil. 1H NMR (CDCl3, 400 MHz) δ 3.40 (s, 3H), 3.51 (brs, 2H), 3.67 (d, 2H, J=4.7 Hz), 4.06 (t, 2H, J=4.7 Hz), 6.32 (d, 1H, J=8.6 Hz), 6.41 (dd, 1H, J=12.6 and 2.8 Hz), and 6.8 (t, 1H, J=9.0 Hz).