HCID 73407283, compound → HCID 17747872, compound

HRID 1160034Notes

Reaction equation

HRID 1160034 reaction equation
[C:1]([O:4][CH:5]([CH2:9][O:10][S:11]([C:14]1[CH:20]=[CH:19][C:17]([CH3:18])=[CH:16][CH:15]=1)(=[O:13])=[O:12])[CH2:6][C:7]#[N:8])(=[O:3])[CH3:2]>C(Cl)(Cl)Cl>[C:1]([O:4][C@@H:5]([CH2:9][O:10][S:11]([C:14]1[CH:20]=[CH:19][C:17]([CH3:18])=[CH:16][CH:15]=1)(=[O:13])=[O:12])[CH2:6][C:7]#[N:8])(=[O:3])[CH3:2]

Participants

3

Reactant 1

HCID 73407283HCID 73407283, compound

Product 1

HCID 17747872HCID 17747872, compoundYield 46%

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

[α]28D=+22.6 (c 1.0, CHCl3); NMR and Mass spectral data are identical to 3-acetyloxy-4-tosyloxybutanenitrile; Yield 46%.

Sources & evidence

ORD record
ord-70256bccbd6d4fc1aac186117c45dd3c
Source dataset
uspto-grants-2010_10
Patent number
US07816119B2

Reaction notes

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