HRID1160136

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID12143105

未命名化合物

结构：CN1C(C)(C)CC(NC(=O)c2ccc(NN)cc2)CC1(C)C

HCID59515576

未命名化合物

PRODUCTS

生成物

结构：Cc1c(-c2ccco2)[nH]n(-c2ccc(C(=O)NC3CC(C)(C)N(C)C(C)(C)C3)cc2)c1=O

HCID59515578

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID176

Acetic Acid

C2H4O2

PROCEDURE

实验过程

3-furan-2-yl-2-methyl-3-oxo-propionic acid ethyl ester (49 mg) and 4-Hydrazino-N-(1,2,2,6,6-pentamethyl-piperidin-4-yl)-benzamide (85 mg) in 0.5 ml of acetic acid were heated up at 65° C. for 2 h. Concentration in vacuo and purification by HPLC gave the expected product. MH+=437.3

WORKUP

后处理

concentrationConcentration
customin vacuo and purification by HPLC