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HRID1160138

反应详情

EQUATION

反应方程式

HRID 1160138 的结构方程式

REACTANTS

反应物

2
结构：CN1C(C)(C)CC(NC(=O)c2ccc(NN)cc2)CC1(C)C
HCID59515576

未命名化合物

结构：CCOC(=O)C(C)(C)C(=O)c1ccco1
HCID59515582

未命名化合物

PRODUCTS

生成物

1
结构：CN1C(C)(C)CC(NC(=O)c2ccc(N3N=C(c4ccco4)C(C)(C)C3=O)cc2)CC1(C)C
HCID59515580

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)O
溶剂HCID176

Acetic Acid

C2H4O2

PROCEDURE

实验过程

3-Furan-2-yl-2,2-dimethyl-3-oxo-propionic acid ethyl ester (53 mg) and 4-Hydrazino-N-(1,2,2,6,6-pentamethyl-piperidin-4-yl)-benzamide (85 mg) in 0.5 ml of acetic acid were heated up at 65° C. for 2 h. Concentration in vacuo and purification by HPLC gave the expected product (MH+: 451.4)

WORKUP

后处理

  1. concentrationConcentration
  2. customin vacuo and purification by HPLC