HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 68691016, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 52258718 | HCID 52258718 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 68691016 | HCID 68691016 | — |
Reaction Steps
68.4 g (0.22 M) of methyl 4-[2-(4-nitrophenoxy)ethoxy]benzoate and 1.3 g of palladium-on-charcoal are added to a mixture of 800 ml of methanol and 200 ml of tetrahydrofuran in a 2000 ml reactor, and the mixture is then maintained under ambient pressure of hydrogen at 60° C. with vigorous stirring for 6 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07816397B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-c786ff198b9f41879788e43b4a45ed14 |
| Source note | uspto-grants-2010_10 |