HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68690903, compound → HCID 68686632, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68690903 | HCID 68690903 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 68686632 | HCID 68686632 | — |
Reaction Steps
8.4 g (0.025 M) of 2-[2-(4-nitrophenoxy)ethoxy]phenylpropanoic acid and 0.9 g of wet 10% palladium-on-charcoal are added to 60 ml of tetrahydrofuran in a 500 ml reactor. The reaction medium is then stirred vigorously for 3 hours under ambient pressure of hydrogen: exothermicity is observed and the temperature of the reaction medium rises to 40° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07816397B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-062fa74ceb7f4e47a7d2488d7ab0f3a2 |
| Source note | uspto-grants-2010_10 |