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HRID1160600

反应详情

EQUATION

反应方程式

HRID 1160600 的结构方程式

REACTANTS

反应物

2
结构：[BH4-].[Na+]
HCID4311764

Sodium borohydride (Na(BH4))

H4BNa

结构：O=C(NCCC[C@H](NC(=O)OCC1c2ccccc2-c2ccccc21)C(=O)O)OCc1ccccc1
HCID14999635

N~5~-[(Benzyloxy)carbonyl]-N~2~-{[(9H-fluoren-9-yl)methoxy]carbonyl}-L-ornithine

C28H28N2O6

PRODUCTS

生成物

1
结构：O=C(NCCC[C@@H](CO)NC(=O)OCC1c2ccccc2-c2ccccc21)OCc1ccccc1
HCID131725891

未命名化合物

PROCEDURE

实验过程

Commercially available Fmoc-Orn(Z) was converted to the alcohol by reduction of its mixed anhydride with sodium borohydride. After crystallization from EtOAc, the compound was thereafter used without further purification.

WORKUP

后处理

  1. customAfter crystallization from EtOAc
  2. customthe compound was thereafter used without further purification