HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 24829988, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | HCID 24829982 | HCID 24829982 | — |
| Catalyst | Osmium Tetroxide | HCID 30318 | — |
| Product | HCID 24829988 | HCID 24829988 | — |
Reaction Steps
A solution of Compound 3 (133 mg, 0.383 mmol) in 2:1 isopropylalcohol and water was stirred at room temperature. N-morpholine oxide (40 mg, 1 eq.) was added followed by a solution of OsO4 (3 mol %). The reaction was stirred for 18 hours, quenched with water and extracted with methylene chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07816535B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-891c818a8b574b909cd24e6dff9ab993 |
| Source note | uspto-grants-2010_10 |