HCID 59518016, compound → HCID 59518023, compound

Participants

Reaction Steps

4′-Butyl-3-nitro-biphenyl-4-ylamine (117 mg, 3.70 mmol) and 10% Pd/C (10 mg) in 2:1 v/v MeOH/EtOAc (4 ml) is treated to a steady bubbling of H2 (g) for 15 minutes. The reaction is kept under 1 atm of H2 for 1 hour with stirring. The reaction is filtered through Celite and the filtrate concentrated in vacuo to afford 4′-butyl-biphenyl-3,4-diamine: ESMS m/z 241.2 (M+H+).

Provenance & Evidence