Cumene → HCID 131728384, compound

HRID 1160847Notes

Reaction equation

HRID 1160847 reaction equation
[C:1]1([CH:7]([CH3:9])[CH3:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:10]=[CH:11][CH3:12]>C1C=CC=CC=1>[CH:7]([C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[CH:11]([CH3:12])[CH3:10])([CH3:9])[CH3:8].[CH:7]([C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)([CH3:9])[CH3:8]

Participants

4

Reactant 2

HCID 7406Cumene2×HCID 8252Propylene

Product 1

HCID 131728384HCID 131728384, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

In these experiments, cumene was manufactured by contacting 5.55 parts by weight benzene and 1 part by weight propylene in the batch slurry reactor using the procedure detailed above for Test Sequence for Cumene Manufacture in a Batch Test over catalyst comprising the 0.127 cm MCM-49 quadrulobal catalyst (Material 1) and the 250 to 297 micron catalyst prepared from it by crushing and sieving (Material 2). Cumene (isopropylbenzene, IPB) and diisopropylbenzene (DIPB) products were collected from each experiment and it was found that Material 2 again provided a 30% reduction in the DIPB/IPB ratio.

Workup

  1. customby crushing
  2. filtrationsieving (Material 2)
  3. customCumene (isopropylbenzene, IPB) and diisopropylbenzene (DIPB) products were collected from each experiment and it

Sources & evidence

ORD record
ord-adcc82a5aaf24efda6afe5d005d19527
Source dataset
uspto-grants-2010_10
Patent number
US07816574B2

Reaction notes

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