1-Bromopentane → HCID 59518046, compound

HRID 1160971Notes

Reaction equation

C[O:2][C:3](=[O:30])[CH2:4][CH2:5][NH:6][C:7](=[O:29])[C:8]1[CH:13]=[CH:12][C:11]([CH:14]([O:21][C:22]2[CH:27]=[CH:26][C:25]([OH:28])=[CH:24][CH:23]=2)[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])=[CH:10][CH:9]=1.Br[CH2:32][CH2:33][CH2:34][CH2:35][CH3:36]>>[CH2:32]([O:28][C:25]1[CH:24]=[CH:23][C:22]([O:21][CH:14]([C:11]2[CH:12]=[CH:13][C:8]([C:7]([NH:6][CH2:5][CH2:4][C:3]([OH:2])=[O:30])=[O:29])=[CH:9][CH:10]=2)[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])=[CH:27][CH:26]=1)[CH2:33][CH2:34][CH2:35][CH3:36]

Participants

Reactant 2

HCID 80571-Bromopentane

HCID 67153488HCID 67153488, compound

Product 1

HCID 59518046HCID 59518046, compound

Procedure

The title compound is prepared in a manner substantially similar to Example 92 starting from 3-{4-[1-(4-hydroxy-phenoxy)-heptyl]-benzoylamino}-propionic acid methyl ester and 1-bromo-pentane. MS: 468.2 [M−H]−.

Sources & evidence

ORD record: ord-126544d8763344d38e6f2a337fc26861
Source dataset: uspto-grants-2010_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07816557B2

Reaction notes

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