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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1161189Generated: October 29, 2026

HCID 59515706, compound → HCID 59515675, compound

https://huagongshe.com/reaction/1161189

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 59515706HCID 59515706—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 59515675HCID 5951567595.5%

Reaction Steps

2-(5-Nitro-1-oxoisoquinolin-2(1H)-yl)ethyl acetate (2.45 g, 0.00842 mol) was dissolved in methanol (100 mL), palladium on charcoal (10%) was added and the reaction mixture was stirred under an atmosphere of hydrogen for 1 hour. The mixture was filtered through celite, and solvent was removed. The product was obtained as a light orange solid (1.98 g). MS m/z=246.5(M+1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07816371B2
Source datasetuspto-grants-2010_10
ORD IDord-3b5e2875cebc4ef08a46e88054be47de
Source noteuspto-grants-2010_10