HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59515706, compound → HCID 59515675, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59515706 | HCID 59515706 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 59515675 | HCID 59515675 | 95.5% |
Reaction Steps
2-(5-Nitro-1-oxoisoquinolin-2(1H)-yl)ethyl acetate (2.45 g, 0.00842 mol) was dissolved in methanol (100 mL), palladium on charcoal (10%) was added and the reaction mixture was stirred under an atmosphere of hydrogen for 1 hour. The mixture was filtered through celite, and solvent was removed. The product was obtained as a light orange solid (1.98 g). MS m/z=246.5(M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07816371B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-3b5e2875cebc4ef08a46e88054be47de |
| Source note | uspto-grants-2010_10 |