HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoic acid, 2-hydrazinyl-, hydrochloride (1:1) → HCID 136173790, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoic acid, 2-hydrazinyl-, hydrochloride (1:1) | HCID 104169 | — |
| Reactant | HCID 72312730 | HCID 72312730 | — |
| Reactant | HCID 72312772 | HCID 72312772 | — |
| Product | HCID 136173790 | HCID 136173790 | 60.2% |
Reaction Steps
The same procedure was carried out as in Example (2f), except that 0.409 g of {2-(3-dimethylcarbamoylmethoxy-5-ethyl-2-fluorophenyl)-2-[4-(5-methyl-[1,2,4]oxadiazol-3-yl)phenylimino]-1-methylsulfanylethylidene}carbamic acid methyl ester and 0.160 g of 2-hydrazinobenzoic acid hydrochloride were used instead of respectively the [2-(4-cyanophenylimino)-2-(2-fluoro-3,5-dimethoxyphenyl)-1-methylsulfanylethylidene]carbamic acid methyl ester and (1-oxypyridin-2-yl)hydrazine, to give the title compound (0.280 g) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07816522B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-196cdda436e041dc9a67937dc446d5cd |
| Source note | uspto-grants-2010_10 |