HuagongsheHuagongshe Chemistry Print Report · For research reference only
Veratraldehyde → {2-(3,4-Dimethoxyphenyl)-1-methylsulfanyl-2-[4-(5-trifluoromethyl-[1,2,4]oxadiazol-3-yl)phenylimino]ethylidene}carbamic acid methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Veratraldehyde | HCID 8419 | — |
| Reactant | 2-Fluoro-4,5-dimethoxybenzaldehyde | HCID 603595 | — |
| Reactant | 4-(5-Methyl-1,2,4-oxadiazol-3-yl)aniline | HCID 18188176 | — |
| Reactant | 4-(5-(Trifluoromethyl)-1,2,4-oxadiazol-3-yl)aniline | HCID 43525144 | — |
| Reactant | [2-(2-Fluoro-4,5-dimethoxyphenyl)-2-[4-(5-methyl-[1,2,4]oxadiazol-3-yl)phenylimino]-1-methylsulfanylethylidene]carbamic acid methyl ester | HCID 72312823 | — |
| Product | {2-(3,4-Dimethoxyphenyl)-1-methylsulfanyl-2-[4-(5-trifluoromethyl-[1,2,4]oxadiazol-3-yl)phenylimino]ethylidene}carbamic acid methyl ester | HCID 72312792 | — |
Reaction Steps
The same procedure was carried out as in Example (1a) to (1d), except that 4-(5-trifluoromethyl-[1,2,4]oxadiazol-3-yl)phenylamine (Example (188a)) and 3,4-dimethoxybenzaldehyde were used instead of respectively 4-(5-methyl-[1,2,4]oxadiazol-3-yl)phenylamine and 2-fluoro-4,5-dimethoxybenzaldehyde in Example (1a), to give the title compound as a light yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07816522B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-b61b81e25aa14125921ea9ab294e253d |
| Source note | uspto-grants-2010_10 |