3,4,5-Trimethoxybenzaldehyde → [2-[4-(5-Methyl-[1,2,4]oxadiazol-3-yl)phenylimino]-1-methylsulfanyl-2-(3,4,5-trimethoxyphenyl)ethylidene]carbamic acid methyl ester

HRID 1161596Notes

Reaction equation

HRID 1161596 reaction equation
[CH3:1][O:2][C:3](=[O:33])[N:4]=[C:5]([S:31][CH3:32])[C:6]([C:20]1[CH:25]=[C:24]([O:26][CH3:27])[C:23]([O:28][CH3:29])=[CH:22][C:21]=1F)=[N:7][C:8]1[CH:13]=[CH:12][C:11]([C:14]2[N:18]=[C:17]([CH3:19])[O:16][N:15]=2)=[CH:10][CH:9]=1.[CH3:34][O:35]C1C=C(C=C(OC)C=1OC)C=O>>[CH3:1][O:2][C:3](=[O:33])[N:4]=[C:5]([S:31][CH3:32])[C:6](=[N:7][C:8]1[CH:13]=[CH:12][C:11]([C:14]2[N:18]=[C:17]([CH3:19])[O:16][N:15]=2)=[CH:10][CH:9]=1)[C:20]1[CH:25]=[C:24]([O:26][CH3:27])[C:23]([O:28][CH3:29])=[C:22]([O:35][CH3:34])[CH:21]=1

Participants

3

Reactant 2

HCID 68583,4,5-TrimethoxybenzaldehydeHCID 72312823[2-(2-Fluoro-4,5-dimethoxyphenyl)-2-[4-(5-methyl-[1,2,4]oxadiazol-3-yl)phenylimino]-1-methylsulfanylethylidene]carbamic acid methyl ester

Product 1

HCID 72312759[2-[4-(5-Methyl-[1,2,4]oxadiazol-3-yl)phenylimino]-1-methylsulfanyl-2-(3,4,5-trimethoxyphenyl)ethylidene]carbamic acid methyl ester

Procedure

The same procedure was carried out as in Examples (1a) to (1d), except that 3,4,5-trimethoxybenzaldehyde was used instead of 2-fluoro-4,5-dimethoxybenzaldehyde in Example (1a), to give the title compound.

Sources & evidence

ORD record
ord-245a93982e3f4e48b237d02561e6d414
Source dataset
uspto-grants-2010_10
Patent number
US07816522B2

Reaction notes

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