HCID 66894201, compound → HCID 66892057, compound

Participants

Reaction Steps

The synthesis was performed according to the procedure of Intermediate 3 starting from 7-piperidin-1-yl-1-benzofuran-5-amine (Intermediate 6). Yield: 70 mg (39%). 1H NMR (400 MHz, CDCl3) δ ppm 1.57-1.62 (m, 2H), 1.70-1.78 (m, 4H), 3.16 (t, 4H), 6.39 (br s, 1H), 6.41 (d, 1H), 6.63 (d, 1H), 6.83 (d, 1H), 7.37-7.43 (m, 2H), 7.49-7.54 (m, 1H), 7.57 (d, 1H), 7.68-7.72 (m, 2H); MS (ESI+) for C19H20N2O3S m/z 357 (M+H)+; HPLC 97% (System A).

Provenance & Evidence