HCID 66893668, compound → HCID 66893170, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure of Intermediate 3 starting from 7-pyrrolidin-1-yl-1-benzofuran-5-amine (Intermediate 9). Yield: 30 mg (22%). 1H NMR (400 MHz, DMSO-d6) δ ppm 1.86-1.93 (m, 4H), 3.36-3.43 (m, 4H), 6.13 (br s, 1H), 6.59 (br s, 1H), 6.73 (d, 1H), 7.45-7.60 (m, 3H), 7.73 (d, 2H), 7.79 (d, 1H), 9.92 (s, 1H); 13C NMR (100 MHz, DMSO-d6) δ ppm 24.73, 48.79, 100.68, 101.51, 106.97, 126.74, 128.33, 129.05, 132.58, 133.70, 134.62, 139.67, 140.68, 145.40; MS (ESI+) for C18H18N2O3S m/z 343 (M+H)+; HPLC 95% (System A).

Provenance & Evidence