HCID 66892653, compound → HCID 66893027, compound

HRID 1162076Notes

Reaction equation

HRID 1162076 reaction equation
CO[C:3]1[CH:8]=[CH:7][C:6](C)=[CH:5][C:4]=1[S:10]([C:13]1[CH:14]=[C:15]([CH2:22][OH:23])[C:16]2[O:20][CH:19]=[CH:18][C:17]=2[CH:21]=1)(=[O:12])=[O:11].C1(S(C2C=C(C(OC)=O)C3OC=CC=3C=2)(=O)=O)C=CC=CC=1>>[C:4]1([S:10]([C:13]2[CH:14]=[C:15]([CH2:22][OH:23])[C:16]3[O:20][CH:19]=[CH:18][C:17]=3[CH:21]=2)(=[O:12])=[O:11])[CH:3]=[CH:8][CH:7]=[CH:6][CH:5]=1

Participants

3

Reactant 2

HCID 66892653HCID 66892653, compoundHCID 66894542HCID 66894542, compound

Product 1

HCID 66893027HCID 66893027, compound

Procedure

The title compound was prepared according to the procedure of Intermediate 68 starting from methyl 5-(phenylsulfonyl)-1-benzofuran-7-carboxylate (80 mg, 0.25 mmol; obtained in Step 2). The crude material was used directly in the subsequent reaction. MS (ESI+) for C15H12O4S m/z 289 (M+H)+.

Sources & evidence

ORD record
ord-14183f2e78294543a9c2ff53f70c35b1
Source dataset
uspto-grants-2010_10
Patent number
US07820675B2

Reaction notes

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