HCID 66891956, compound → HCID 66894479, compound

HRID 1162078Notes

Reaction equation

HRID 1162078 reaction equation
COC1C=CC(C)=CC=1S(C1C=C(CO)C2OC=CC=2C=1)(=O)=O.[CH3:24][C:25]1[CH:30]=[CH:29][C:28]([S:31]([C:34]2[CH:35]=[C:36]([C:43](OC)=[O:44])[C:37]3[O:41][CH:40]=[CH:39][C:38]=3[CH:42]=2)(=[O:33])=[O:32])=[CH:27][CH:26]=1>>[CH3:24][C:25]1[CH:26]=[CH:27][C:28]([S:31]([C:34]2[CH:35]=[C:36]([CH2:43][OH:44])[C:37]3[O:41][CH:40]=[CH:39][C:38]=3[CH:42]=2)(=[O:33])=[O:32])=[CH:29][CH:30]=1

Participants

3

Reactant 2

HCID 66891956HCID 66891956, compoundHCID 66894542HCID 66894542, compound

Product 1

HCID 66894479HCID 66894479, compound

Procedure

The title compound was prepared according to the procedure of Intermediate 68 starting from methyl 5-[(4-methylphenyl)sulfonyl]-1-benzofuran-7-carboxylate (62 mg, 0.19 mmol; obtained in Step 2). MS (ESI+) for C16H14O4S m/z 303 (M+H)+.

Sources & evidence

ORD record
ord-061991e116a347c998d3882f1208ac34
Source dataset
uspto-grants-2010_10
Patent number
US07820675B2

Reaction notes

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