HRID1162396

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID22499186

未命名化合物

结构：CC(=O)c1ccc2c(c1)CC(C)(NC(=O)c1ccccc1)C2

HCID22499217

未命名化合物

PRODUCTS

生成物

HCID22499186

未命名化合物

结构：CCc1cc2c(cc1C(C)=O)CC(C)(NC(=O)c1ccccc1)C2

HCID22499225

未命名化合物

PROCEDURE

实验过程

N-(5-Acetyl-6-ethyl-2-methyl-indan-2-yl)-benzamide is prepared from N-(5-ethyl-2-methyl-indan-2-yl)-benzamide (2.6 g) following the procedure used to prepare N-(5-acetyl-2-methyl-indan-2-yl)-benzamide. The product is purified by chromatography (silica, hexane/ethyl acetate, 4:1) to give the title compound. ES+ MS m/e 322 (MH+)

WORKUP

后处理

customThe product is purified by chromatography (silica, hexane/ethyl acetate, 4:1)

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-44f9d867cfe74a319faa66db8604c592
来源数据集: uspto-grants-2010_10
DOI: 10.6084/m9.figshare.5104873.v1
专利: US07820694B2
来源说明: uspto-grants-2010_10

反应 SMILES

[CH2:1]([C:3]1[CH:4]=[C:5]2[C:9](=[CH:10][CH:11]=1)[CH2:8][C:7]([NH:13][C:14](=[O:21])[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)([CH3:12])[CH2:6]2)[CH3:2].[C:22]([C:25]1[CH:26]=[C:27]2[C:31](=[CH:32][CH:33]=1)[CH2:30][C:29]([NH:35][C:36](=[O:43])[C:37]1[CH:42]=[CH:41][CH:40]=[CH:39][CH:38]=1)([CH3:34])[CH2:28]2)(=[O:24])[CH3:23]>>[C:22]([C:11]1[CH:10]=[C:9]2[C:5](=[CH:4][C:3]=1[CH2:1][CH3:2])[CH2:6][C:7]([NH:13][C:14](=[O:21])[C:15]1[CH:16]=[CH:17][CH:18]=[CH:19][CH:20]=1)([CH3:12])[CH2:8]2)(=[O:24])[CH3:23].[CH2:22]([C:25]1[CH:26]=[C:27]2[C:31](=[CH:32][CH:33]=1)[CH2:30][C:29]([NH:35][C:36](=[O:43])[C:37]1[CH:38]=[CH:39][CH:40]=[CH:41][CH:42]=1)([CH3:34])[CH2:28]2)[CH3:23]