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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1163041Generated: October 28, 2026

6-Bromohexanoic acid → HCID 178433620, compound

https://huagongshe.com/reaction/1163041

Reaction equation

Participants

RoleNameHCIDCharge
Reactant6-Bromohexanoic acidHCID 20210—
Reactant2,3,3-Trimethyl-3H-pyrrolo[2,3-b]pyridineHCID 22266836—
SolventEthyl AcetateHCID 8857—
ProductHCID 178433620HCID 178433620—

Reaction Conditions

Temperature120 °C

Reaction Steps

A mixture of 0.54 g of 2,3,3-trimethyl-3H-pyrrolo[2,3-b]pyridine and 1.32 g of 6-bromohexanoic acid is heated at 120° C. for one hour. Ethyl acetate (10 mL) is added, and the reaction mixture is heated at reflux for 15 minutes, then cooled to room temperature. The supernatant liquid is decanted to yield the product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07820824B2
Source datasetuspto-grants-2010_10
ORD IDord-86feff4f2ce947e9856af863eb1da3a6
Source noteuspto-grants-2010_10