HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoic acid, 4-amino-3-nitro- → HCID 68443031, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoic acid, 4-amino-3-nitro- | HCID 74115 | — |
| Reactant | 1H-Indazol-6-amine | HCID 81423 | — |
| Reactant | Methanaminium, N-((1H-benzotriazol-1-yloxy)(dimethylamino)methylene)-N-methyl-, hexafluorophosphate(1-) (1:1) | HCID 2733084 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 68443031 | HCID 68443031 | — |
Reaction Steps
4-Amino-3-nitrobenzoic acid (27 mmol) was coupled with 6-aminoindazole (30 mmol) using HBTU (30 mmol) in dry DMF as the solvent employing the general procedure D to afford 4-amino-N-(1H-indazol-6-yl)-3-nitrobenzamide which was used for further transformation without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07820821B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-fefd4d82adef4830824f07fd6505afd4 |
| Source note | uspto-grants-2010_10 |