HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-aminobenzoate → HCID 22060542, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-aminobenzoate | HCID 11400 | — |
| Reactant | 2,4-Dichloro-5-fluoropyrimidine | HCID 250705 | — |
| Product | HCID 22060542 | HCID 22060542 | — |
Reaction Steps
In like manner to the preparation of N2,N4-bis(3-hydroxyphenyl)-5-fluoro-2,4-pyrimidinediamine, the reaction of 2,4-dichloro-5-fluoropyrimidine and 3-ethoxycarbonylaniline gave N2,N4-bis(3-ethoxycarbonylphenyl)-5-fluoro-2,4-pyrimidinediamine. LCMS: ret. time: 26.55 min.; purity: 100%; MS (m/e): 425 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07820819B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-424fd985a16d423983cab047439f083a |
| Source note | uspto-grants-2010_10 |