Isopropylamine → HCID 53827821, compound

HRID 1163895Notes

Reaction equation

HRID 1163895 reaction equation
[O:1]1[CH2:16][CH:2]1[CH2:3][O:4][C:5]1[CH:11]=[C:10]([CH3:12])[CH:9]=[C:8]([N+:13]([O-:15])=[O:14])[C:6]=1[NH2:7].[CH3:17][CH:18]([NH2:20])[CH3:19]>>[OH:1][CH:2]([CH2:16][NH:20][CH:18]([CH3:19])[CH3:17])[CH2:3][O:4][C:5]1[CH:11]=[C:10]([CH3:12])[CH:9]=[C:8]([N+:13]([O-:15])=[O:14])[C:6]=1[NH2:7]

Participants

3

Reactant 2

HCID 6363IsopropylamineHCID 20467867HCID 20467867, compound

Product 1

HCID 53827821HCID 53827821, compound

Procedure

The diamine used as intermediate is obtained by reacting the 2-(2,3-epoxypropoxy)-4-methyl-6-nitroaniline described in Example 1 with 2-propylamine to give 2-[2-hydroxy-3-(2-propylamino)-propoxy]-4-methyl-6-nitroaniline, which is then subjected to catalytic hydrogenation.

Workup

  1. customis obtained

Sources & evidence

ORD record
ord-1c52e624bdf54dd2b3297b662a3500b4
Source dataset
uspto-grants-1983_01
Patent number
US04367235

Reaction notes

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