Ethanol → HCID 20513296, compound

HRID 1163901Notes

Reaction equation

HRID 1163901 reaction equation
[NH2:1][C:2]1[C:7]([N+:8]([O-])=O)=[C:6]([CH3:11])[C:5]([CH3:12])=[CH:4][C:3]=1[O:13][CH2:14][CH:15]1[O:17][CH2:16]1.[CH3:18][CH:19]([NH2:21])[CH3:20].[CH2:22]([OH:24])C>>[CH3:12][C:5]1[CH:4]=[C:3]([O:13][CH2:14][CH:15]([OH:17])[CH2:16][NH:21][CH:19]([CH3:20])[CH3:18])[C:2]2[NH:1][C:22](=[O:24])[NH:8][C:7]=2[C:6]=1[CH3:11]

Participants

4

Reactant 3

HCID 702EthanolHCID 6363IsopropylamineHCID 20513319HCID 20513319, compound

Product 1

HCID 20513296HCID 20513296, compound

Procedure

The diamino compound used as intermediate is obtained by reacting 2-amino-4,5-dimethyl-1-(2,3-epoxypropoxy)-3-nitrobenzene (see Example 8) with 2-propylamine in boiling ethanol and subsequent catalytic hydrogenation.

Workup

  1. customis obtained

Sources & evidence

ORD record
ord-aa0332c60ba44e03a5d426afe93e512c
Source dataset
uspto-grants-1983_01
Patent number
US04367235

Reaction notes

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