Potassium thiocyanate → HCID 20461213, compound

HRID 1163906Notes

Reaction equation

HRID 1163906 reaction equation
Cl.[NH2:2][CH:3]([C:7](=[O:10])[CH2:8][CH3:9])[C:4](=O)[CH3:5].[S-:11][C:12]#[N:13].[K+]>O>[CH3:5][C:4]1[NH:13][C:12](=[S:11])[NH:2][C:3]=1[C:7](=[O:10])[CH2:8][CH3:9]

Participants

4

Reactant 2

HCID 516872Potassium thiocyanateHCID 20461222HCID 20461222, compound

Product 1

HCID 20461213HCID 20461213, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Ten grams of 3-amino-2,4-hexanedione hydrochloride are dissolved in 100 ml water. Fifteen grams of potassium thiocyanate are added and the mixture is heated on the steam bath for 10 minutes. On cooling, the title compound is obtained.

Workup

  1. temperaturethe mixture is heated on the steam bath for 10 minutes
  2. temperatureOn cooling

Sources & evidence

ORD record
ord-9fc68e233fc54de697ae1d4a40f20217
Source dataset
uspto-grants-1983_01
Patent number
US04367236

Reaction notes

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