Azobisisobutyronitrile → HCID 20513437, compound

Participants

Reaction Steps

A mixture of 4-chlorophenyl 2-methoxy-3-methylphenyl ether (10.7 g), N-bromosuccinimide (8.3 g) and 2,2'-azobisisobutyronitrile (830 mg) in benzene (70 ml) was refluxed under heating for 2 hrs., and the reaction mixture was treated in a similar manner to that of Example 5-(3) to give oily 4-chlorophenyl 2-methoxy-3-bromomethylphenyl ether (14.9 g).

Provenance & Evidence