Dimethyl Sulfate → HCID 20513489, compound

HRID 1164010Notes

Reaction equation

HRID 1164010 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:14]=[CH:15][CH:16]=1)[O:5][C:6]1[CH:7]=[CH:8][CH:9]=[C:10]([CH3:13])[C:11]=1[OH:12].S(OC)(O[CH3:21])(=O)=O>[OH-].[Na+]>[CH3:21][O:12][C:11]1[C:10]([CH3:13])=[CH:9][CH:8]=[CH:7][C:6]=1[O:5][C:4]1[CH:14]=[CH:15][CH:16]=[C:2]([Cl:1])[CH:3]=1

Participants

4

Reactant 2

HCID 6497Dimethyl SulfateHCID 205135046-(3-Chlorophenoxy)-o-cresol

Product 1

HCID 20513489HCID 20513489, compound

Reagents, catalysts & solvents 1

HCID 14798Sodium HydroxideSolvent

Procedure

An aqueous solution (40 ml) of sodium hydroxide (10 g) and a mixture of 6-(3-chlorophenoxy)-o-cresol (13.9 g) and dimethyl sulfate (11 ml) were treated in a similar manner to that of Example 6-(2) to give oily 3-chlorophenyl 2-methoxy-3-methylphenyl ether (14.6 g).

Workup

  1. additionwere treated in a similar manner to that of Example 6-(2)

Sources & evidence

ORD record
ord-56aaacb8ebb94e23abcb46152d18fc18
Source dataset
uspto-grants-1983_01
Patent number
US04367238

Reaction notes

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