HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Bromide → Ethyl 2-cyano-2-[2-methoxy-3-(2-chlorophenoxy)phenyl]butyrate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Bromide | HCID 6332 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 20513486 | HCID 20513486 | — |
| Product | Ethyl 2-cyano-2-[2-methoxy-3-(2-chlorophenoxy)phenyl]butyrate | HCID 20513442 | 91% |
Reaction Steps
Sodium hydride (50%, 920 mg), ethyl 2-cyano-2-[2-methoxy-3-(2-chlorophenoxy)phenyl]acetate (6 g) and ethyl bromide (2.84 g) were treated in a similar manner to that of Example 10-(5) to give oily ethyl 2-cyano-2-[2-methoxy-3-(2-chlorophenoxy)phenyl]butyrate (5.9 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04367238 |
| Source dataset | uspto-grants-1983_01 |
| ORD ID | ord-a1fcee1a3f1e409e8d6f0250e2af431b |
| Source note | uspto-grants-1983_01 |