HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → Phenyl 2-methoxy-3-methylphenyl ether
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 6-Phenoxy-o-cresol | HCID 22734681 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Phenyl 2-methoxy-3-methylphenyl ether | HCID 20082997 | 74.8% |
Reaction Steps
A mixture of 6-phenoxy-o-cresol (7.5 g) and dimethyl sulfate (14 g) and aqueous solution (30 ml) of potassium hydroxide (10.5 g) were treated in a similar manner to that of Example 14-(2). The resultant residue was pulverized with ethanol to give phenyl 2-methoxy-3-methylphenyl ether (6 g). mp 52°-53° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04367238 |
| Source dataset | uspto-grants-1983_01 |
| ORD ID | ord-1184ecfe4267478496a28147cca519d9 |
| Source note | uspto-grants-1983_01 |