HRID1164089
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
To a suspension of 2-hydroxy-3-(2-chlorophenylthio)benzaldehyde (5.8 g) in methanol (50 ml) was added sodium borohydride (820 mg) at temperature below 15° C. with stirring. The mixture was treated in a similar manner to that of Example 21-(5) to give oily 2-hydroxy-3-(2-chlorophenylthio)benzyl alcohol (6 g). This oily substance was left to stand at room temperature to give crystals.
WORKUP
后处理
- additionThe mixture was treated in a similar manner to that of Example 21-(5)