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HRID1164411

反应详情

EQUATION

反应方程式

HRID 1164411 的结构方程式

REACTANTS

反应物

3
结构：CCOC(=O)Cl
HCID10928

Ethyl chloroformate

C3H5ClO2

结构：[Na+].[OH-]
HCID14798

Sodium Hydroxide

HNaO

结构：CC1(C)CC(NC2CC(C)(C)NC(C)(C)C2)CC(C)(C)N1
HCID566708

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)N(C1CC(C)(C)NC(C)(C)C1)C1CC(C)(C)NC(C)(C)C1
HCID20277459

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClC(Cl)Cl
溶剂HCID6212

Chloroform

CHCl3

PROCEDURE

实验过程

The N-ethoxycarbonyl-bis(2,2,6,6-tetramethyl-4-piperidyl)-amine is prepared by reacting bis(2,2,6,6-tetramethyl-4-piperidyl)-amine with ethyl chlorocarbonate in chloroform at 10°-20° C. in the presence of aqueous NaOH. The product obtained, which has a purity of 99.2% and melts at 117° C., can be used directly.

WORKUP

后处理

  1. customat 10°-20° C.
  2. customThe product obtained