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HRID1164414

反应详情

EQUATION

反应方程式

HRID 1164414 的结构方程式

REACTANTS

反应物

3
结构：O=C1C=CC(=O)O1
HCID7923

2,5-Furandione

C4H2O3

结构：CC(=O)C1=C(C)CCCC1(C)C
HCID539316

1-(2,6,6-Trimethyl-1-cyclohexen-1-yl)ethanone

C11H18O

结构：[H][H]
HCID178418361

未命名化合物

PRODUCTS

生成物

1
结构：CC(=O)C12OC1(C)CCCC2(C)C
HCID20512484

1-(2,2,6-Trimethyl-7-oxabicyclo[4.1.0]heptan-1-yl)ethan-1-one

C11H18O2

收率 95%

PROCEDURE

实验过程

8.3 g (0.05 M) of 2,6,6-trimethyl-cyclohex-1-enyl methyl ketone have been treated with maleic anhydride and hydrogen peroxyde according to Example 1, to give, after extraction and purification as described above, 8.5 g (yield 95%) of the desired product, b.p. 85°/6 Torr:

WORKUP

后处理

  1. customto give
  2. extractionafter extraction and purification