HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propylene Oxide → N-(beta-hydroxypropyl)-2-chloro-6-methyl-aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propylene Oxide | HCID 6378 | — |
| Reactant | 2-Chloro-6-methylaniline | HCID 6897 | — |
| Product | N-(beta-hydroxypropyl)-2-chloro-6-methyl-aniline | HCID 13674766 | 30.1% |
Reaction Steps
2-Chloro-6-methyl-aniline is reacted with 1,2-epoxypropane as described in Example 3, Method (b), point (a) to obtain N-(β-hydroxypropyl)-2-chloro-6-methyl-aniline with a yield of 30.1%; b.p.: 118°-122° C./0.2 mm Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04369325 |
| Source dataset | uspto-grants-1983_01 |
| ORD ID | ord-ac32e516765a482eaf631e962e822a1c |
| Source note | uspto-grants-1983_01 |