Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Isobutylene → 1,3,3-Trimethyl-1-phenylindan-5-ol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Isobutylene | HCID 8255 | — |
| 반응물 | 4-(1-Phenylethyl)phenol | HCID 94763 | — |
| 생성물 | 1,3,3-Trimethyl-1-phenylindan-5-ol | HCID 103816 | 13.5% |
반응 단계
112 g of isobutylene were introduced with stirring into 198 g of 1-phenyl-1-(4-hydroxy-phenyl)-ethane and 30 g of an acid activated Fuller's earth at 150° C. and the reaction mixture was then stirred at this temperature for 5 hours. 34 g of 1,3,3-trimethyl-1-phenyl-5-hydroxy-indane could be obtained by distillation followed by recrystallisation.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04370505 |
| 출처 데이터셋 | uspto-grants-1983_01 |
| ORD ID | ord-550c557410dd4c56bae252d5eb160f99 |
| 출처 메모 | uspto-grants-1983_01 |