HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → 4-(4-Octyloxyphenyl)benzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 4'-(Octyloxy)-[1,1'-biphenyl]-4-carboxylic acid | HCID 2802556 | — |
| Product | 4-(4-Octyloxyphenyl)benzoyl chloride | HCID 11078473 | — |
Reaction Steps
4-[4-Octyloxyphenyl]benzoic acid (OPBA) was converted into its acid chloride, OPBC, by heating it at reflux with oxalyl chloride after which excess oxalyl chloride was allowed to distil out and the residue taken up in ethanol free chloroform.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04906402 |
| Source dataset | uspto-grants-1990_03 |
| ORD ID | ord-5cd4bfd498614178a93744859f51562d |
| Source note | uspto-grants-1990_03 |