Chloroacetyl chloride → HCID 19863424, compound

HRID 1164944Notes

Reaction equation

HRID 1164944 reaction equation
[CH:1]1([CH2:6][CH2:7][N:8]([CH2:22][C:23]2C=CC=CC=2)[CH2:9][CH2:10][CH2:11][NH:12][C:13]2[CH:18]=[CH:17][C:16]([N+:19]([O-:21])=[O:20])=[CH:15][CH:14]=2)[CH2:5][CH2:4][CH2:3][CH2:2]1.ClCC(Cl)=[O:32]>>[CH:1]1([CH2:6][CH2:7][N:8]2[CH2:9][CH2:10][CH2:11][N:12]([C:13]3[CH:14]=[CH:15][C:16]([N+:19]([O-:21])=[O:20])=[CH:17][CH:18]=3)[C:23](=[O:32])[CH2:22]2)[CH2:2][CH2:3][CH2:4][CH2:5]1

Participants

3

Reactant 2

HCID 6577Chloroacetyl chlorideHCID 53700404HCID 53700404, compound

Product 1

HCID 19863424HCID 19863424, compound

Procedure

In a manner similar to Preparation 13 react N-[2 (cyclopentyl)ethyl]-N'-(4-nitrophenyl)-N-(phenylmethyl)1,3-propanediamine with chloroacetyl chloride to obtain the title compound.

Workup

  1. customIn a manner similar to Preparation 13

Sources & evidence

ORD record
ord-2e883a0dffcc40aaa317f91a2279a268
Source dataset
uspto-grants-1990_03
Patent number
US04906634

Reaction notes

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