HCID 19863391, compound → HCID 19863467, compound

HRID 1164960Notes

Reaction equation

HRID 1164960 reaction equation
[ClH:1].[CH2:2]([N:4]([CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24])[CH2:5][CH2:6][CH2:7][O:8][C:9]1[CH:14]=[CH:13][C:12]([N+:15]([O-])=O)=[CH:11][CH:10]=1)[CH3:3]>[Pd].CO>[ClH:1].[ClH:1].[CH2:2]([N:4]([CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24])[CH2:5][CH2:6][CH2:7][O:8][C:9]1[CH:10]=[CH:11][C:12]([NH2:15])=[CH:13][CH:14]=1)[CH3:3]

Participants

4

Reactant 1

HCID 19863391HCID 19863391, compound

Product 1

HCID 19863467HCID 19863467, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 887MethanolSolvent

Procedure

In a manner similar to Preparation 42 hydrogenate N-ethyl-N-heptyl-3-(4-nitrophenoxy)propanamine hydrochloride over 10% palladium on carbon in methanol to obtain the title compound.

Sources & evidence

ORD record
ord-dcf6f1ca498b4821b9bed482c3356a6f
Source dataset
uspto-grants-1990_03
Patent number
US04906634

Reaction notes

Loading…