5-Fluoro-2-nitrotoluene → HCID 19863386, compound
Reaction equation
F[C:2]1[CH:3]=[CH:4][C:5]([N+:9]([O-:11])=[O:10])=[C:6]([CH3:8])[CH:7]=1.[CH3:12][CH:13]([N:15]([CH:20]([CH3:22])[CH3:21])[CH2:16][CH2:17][CH2:18][SH:19])[CH3:14]>>[CH3:8][C:6]1[CH:7]=[C:2]([S:19][CH2:18][CH2:17][CH2:16][N:15]([CH:20]([CH3:22])[CH3:21])[CH:13]([CH3:12])[CH3:14])[CH:3]=[CH:4][C:5]=1[N+:9]([O-:11])=[O:10]Participants
3
Procedure
In a manner similar to Preparation 43 react 5-fluoro-2-nitrotoluene with 3-[bis(1-methylethyl)amino]propanethiol to obtain the tile compound.
Workup
- customIn a manner similar to Preparation 43
- customto obtain the tile compound
Sources & evidence
- ORD record
- ord-ff04912f242d419794b383aff038a68a
- Source dataset
- uspto-grants-1990_03
- Patent number
- US04906634
Reaction notes
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