Stannous Chloride → HCID 19863383, compound

HRID 1164963Notes

Reaction equation

HRID 1164963 reaction equation
[CH3:1][C:2]1[CH:3]=[C:4]([S:11][CH2:12][CH2:13][CH2:14][N:15]([CH:19]([CH3:21])[CH3:20])[CH:16]([CH3:18])[CH3:17])[CH:5]=[CH:6][C:7]=1[N+:8]([O-])=O.[Sn](Cl)Cl>C(O)C>[CH3:1][C:2]1[CH:3]=[C:4]([S:11][CH2:12][CH2:13][CH2:14][N:15]([CH:16]([CH3:18])[CH3:17])[CH:19]([CH3:20])[CH3:21])[CH:5]=[CH:6][C:7]=1[NH2:8]

Participants

4

Reactant 2

HCID 24479Stannous ChlorideHCID 19863386HCID 19863386, compound

Product 1

HCID 19863383HCID 19863383, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

In a manner similar to Preparation 39 react 3-[(3-methyl-4-nitrophenyl)thio]-N,N-bis(1-methylethyl)propanamine with tin(11) chloride in ethanol to obtain the title compound.

Workup

  1. customIn a manner similar to Preparation 39

Sources & evidence

ORD record
ord-c1ca93b1b40243489d808e97bb2aa8d9
Source dataset
uspto-grants-1990_03
Patent number
US04906634

Reaction notes

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