N-Methylhomoveratrylamine → HCID 9976678, compound

HRID 1164970Notes

Reaction equation

HRID 1164970 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH2:11][CH2:12][NH:13][CH3:14])[CH:6]=[CH:7][C:8]=1[O:9][CH3:10].Cl[CH2:16][CH2:17][CH2:18][O:19][C:20]1[CH:25]=[CH:24][C:23]([N+:26]([O-:28])=[O:27])=[CH:22][CH:21]=1>C(#N)C>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH2:11][CH2:12][N:13]([CH2:16][CH2:17][CH2:18][O:19][C:20]2[CH:25]=[CH:24][C:23]([N+:26]([O-:28])=[O:27])=[CH:22][CH:21]=2)[CH3:14])[CH:6]=[CH:7][C:8]=1[O:9][CH3:10]

Participants

4

Reactant 2

HCID 77039N-MethylhomoveratrylamineHCID 118446171-(3-Chloropropoxy)-4-nitrobenzene

Product 1

HCID 9976678HCID 9976678, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

In a manner similar to Preparation 56 react 3,4-dimethoxy-N-methylbenzeneethanamine with 1-(3-chloropropoxy)-4-nitrobenzene in acetonitrile to obtain the title compound.

Workup

  1. customIn a manner similar to Preparation 56

Sources & evidence

ORD record
ord-452a9f70f50b439caa5053cfd836c5a8
Source dataset
uspto-grants-1990_03
Patent number
US04906634

Reaction notes

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