HCID 19863362, compound → HCID 19863436, compound

HRID 1164977Notes

Reaction equation

HRID 1164977 reaction equation
[CH:1]1([CH2:6][CH2:7][N:8]2[CH2:14][CH2:13][CH2:12][N:11]([C:15]3[CH:20]=[CH:19][C:18]([NH:21][S:22]([CH3:25])(=[O:24])=[O:23])=[CH:17][CH:16]=3)[C:10](=O)[CH2:9]2)[CH2:5][CH2:4][CH2:3][CH2:2]1.[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[CH:1]1([CH2:6][CH2:7][N:8]2[CH2:14][CH2:13][CH2:12][N:11]([C:15]3[CH:16]=[CH:17][C:18]([NH:21][S:22]([CH3:25])(=[O:23])=[O:24])=[CH:19][CH:20]=3)[CH2:10][CH2:9]2)[CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 19863362HCID 19863362, compoundHCID 21226445Aluminium lithium hydride

Product 1

HCID 19863436HCID 19863436, compound

Procedure

In a manner similar to Example 1 react N-[4-[4-(2-[cyclopentyl)ethyl]hexahydro-2-oxo-1H-1,4-diazepin-1-yl]phenyl]methanesulfonamide with lithium aluminum hydride to obtain the title compound.

Sources & evidence

ORD record
ord-34d169a0b9104bbf9660718eca9ac033
Source dataset
uspto-grants-1990_03
Patent number
US04906634

Reaction notes

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