HCID 19863368, compound → HCID 19863453, compound

HRID 1164978Notes

Reaction equation

HRID 1164978 reaction equation
[CH:1]1([CH2:7][CH2:8][NH:9][CH:10]([CH2:34][CH3:35])[CH2:11][CH2:12][C:13]([N:15]([C:23]2[CH:28]=[CH:27][C:26]([NH:29][S:30]([CH3:33])(=[O:32])=[O:31])=[CH:25][CH:24]=2)[CH2:16][C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)=O)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[CH:1]1([CH2:7][CH2:8][NH:9][CH:10]([CH2:34][CH3:35])[CH2:11][CH2:12][CH2:13][N:15]([CH2:16][C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[C:23]2[CH:24]=[CH:25][C:26]([NH:29][S:30]([CH3:33])(=[O:31])=[O:32])=[CH:27][CH:28]=2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 19863368HCID 19863368, compoundHCID 21226445Aluminium lithium hydride

Product 1

HCID 19863453HCID 19863453, compound

Procedure

In a manner similar to Example 1 react 4-[[2-(cyclohexyl)ethyl]amino]-N-[4-[(methylsulfonyl)amino]phenyl]-N-(phenylmethyl)hexanamide with lithium aluminum hydride to obtain the title compound.

Sources & evidence

ORD record
ord-58ba6db8fd854410be925b9443a0be48
Source dataset
uspto-grants-1990_03
Patent number
US04906634

Reaction notes

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