Ethyl 2-bromopropionate → HCID 178472295, compound

HRID 1165187Notes

Reaction equation

HRID 1165187 reaction equation
[SH:1][C:2]1[S:3][C:4]([SH:7])=[N:5][N:6]=1.Br[CH:9]([CH3:15])[C:10]([O:12][CH2:13][CH3:14])=[O:11]>>[SH:7][C:4]1[S:3][C:2]([S:1][CH:9]([CH3:15])[C:10]([O:12][CH2:13][CH3:14])=[O:11])=[N:6][N:5]=1

Participants

3

Reactant 2

HCID 79040Ethyl 2-bromopropionateHCID 178418558HCID 178418558, compound

Product 1

HCID 178472295HCID 178472295, compoundYield 76%

Procedure

By following the same procedure as Reference Example 6 using 7.5 g of 2,5-dimercapto-1,3,4-thiadiazole and 5.8 g of ethyl 2-bromopropionate as the starting materials, 6.1 g of ethyl 2-[(5-mercapto-1,3,4-thiadiazol-2-yl)thio]propionate was obtained as an oily product.

Sources & evidence

ORD record
ord-491b70c817954ef4ac8216aff2c2e918
Source dataset
uspto-grants-1990_03
Patent number
US04908368

Reaction notes

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