HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Ethyl Ketone → 2-(4-Pentoxyphenoxymethyl)oxirane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Ethyl Ketone | HCID 6569 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | p-Pentyloxyphenol | HCID 29353 | — |
| Product | 2-(4-Pentoxyphenoxymethyl)oxirane | HCID 14748276 | — |
Reaction Steps
A mixture of 24.41 g of 4-pentoxyphenol, 56 g of K2CO3, 34.7 ml of epicholorohydrin and 500 ml of methyl ethyl ketone was refluxed overnight. Solvent and solid were removed to yield a residue which was distilled by a Kugelrohr adaptor to give the title compound, bp 175°/0.01 mmHg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04908384 |
| Source dataset | uspto-grants-1990_03 |
| ORD ID | ord-59355c75c4a64e0a8ce9825ac7fd3871 |
| Source note | uspto-grants-1990_03 |