Butylamine → Pyrrolidine, 1-butyl-
Reaction equation
[CH2:1](O)[CH2:2][CH2:3][CH2:4]O.[CH2:7]([NH2:11])[CH2:8][CH2:9][CH3:10]>>[CH2:1]([N:11]1[CH2:10][CH2:9][CH2:8][CH2:7]1)[CH2:2][CH2:3][CH3:4]Participants
3
Procedure
11.7 kg of butane-1,4-diol were reacted with 7.3 kg of n-butylamine similarly to Example 1. N-(n-butyl)-pyrrolidine was obtained in 96% yield.
Sources & evidence
- ORD record
- ord-5734087ff5894d6b86d0c41b5885d86f
- Source dataset
- uspto-grants-1990_03
- Patent number
- US04910304
Reaction notes
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