Sodium Hydroxide → HCID 19064119, compound

HRID 1165611Notes

Reaction equation

[OH:1][CH2:2][CH2:3][CH2:4][NH:5][C:6]1[CH:11]=[CH:10][C:9]([N:12]2[C:16](=O)[CH2:15][O:14][CH-]2)=[CH:8][C:7]=1[N+:18]([O-:20])=[O:19].[OH-].[Na+]>>[OH:1][CH2:2][CH2:3][CH2:4][NH:5][C:6]1[CH:11]=[CH:10][C:9]([NH:12][CH2:16][CH2:15][OH:14])=[CH:8][C:7]=1[N+:18]([O-:20])=[O:19]

Participants

Reactant 2

HCID 14798Sodium Hydroxide

HCID 178516899HCID 178516899, compound

Product 1

HCID 19064119HCID 19064119, compound

Conditions

Temperature: 80 °C

Procedure

0.02 mole (5.1 g) of N-[4-(γ-hydroxypropyl)amino-3-nitrophenyl]oxazolidone, prepared according to Example 6 or 8, is added to 22 moles of 2N sodium hydroxide. After 30 minutes' heating at 80° C., the expected product crystallizes from the reaction medium.

Workup

customthe expected product crystallizes from the reaction medium

Sources & evidence

ORD record: ord-30111050a67c4157930d41c2d68ac6e4
Source dataset: uspto-grants-1990_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04910341

Reaction notes

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